4-Methoxybenzaldehyde → S-ethyl (E)-3-(4-methoxyphenyl)prop-2-enethioate
Reaktionsgleichung
COc1ccc(C=O)cc1.CCSC(=O)CC(=O)O>NCc1ccccc1.O=C(O)C(F)(F)F.CN(C)c1ccncc1.CN(C)C=O>CCSC(=O)/C=C/c1ccc(OC)cc1Komponenten
6
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 3
Reaktionsbedingungen
- Temperatur
- 25 °C
Aufarbeitung
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic-Phase beibehalten
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
Quellen und Nachweise
- ORD-Eintrag
- ord-d98c486ba3ae4b90868aae8de0a673dc
- Quelldatensatz
- Bayesian optimization of 5 decarboxylative olefination reactions
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