Butanal → 56249-61-7

HRID 1828213Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1828213
[CH:1](=O)[CH2:2][CH2:3][CH3:4].[CH2:6]([NH2:13])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C1(C)C=CC=CC=1>[CH:1](=[N:13][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH2:2][CH2:3][CH3:4]

Komponenten

4

Edukt 2

HCID 261ButanalHCID 7504Benzylamine

Produkt 1

HCID 455591156249-61-7

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

This material is a known compound prepared in the standard fashion. To about 100 mL of toluene was added 28 mL of butyraldehyde, 34 mL of benzylamine, and several grams of 3A molecular sieves. The mixture became warm and turbid after standing for a few minutes. After standing for several hours the mixture was colorless and transparent. The imine product was isolated by distillation under vacuum and characterized by NMR spectroscopy.

Aufarbeitung

  1. customprepared in the standard fashion
  2. temperatureThe mixture became warm
  3. waitafter standing for a few minutes
  4. waitAfter standing for several hours

Quellen und Nachweise

ORD-Eintrag
ord-7e2557d71c324fc2afdd4937f6cdf32b
Quelldatensatz
uspto-grants-2006_06
Patentnummer
US07056979B1

Notizen zur Reaktion

Wird geladen…