N-(1-pyridin-4-ylethyl)formamide → HCID 22052374, Verbindung

HRID 1831807Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1831807
[N:1]1[CH:6]=[CH:5][C:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])=[CH:3][CH:2]=1.[H][H]>C(O)(=O)C>[NH:1]1[CH2:6][CH2:5][CH:4]([CH:7]([NH:9][CH:10]=[O:11])[CH3:8])[CH2:3][CH2:2]1

Komponenten

4

Edukt 2

HCID 2771720N-(1-pyridin-4-ylethyl)formamideHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 22052374HCID 22052374, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 176Acetic AcidLösungsmittel

Versuchsvorschrift

N-(1-Pyridin-4-yl-ethyl)-formamide (1.86 g, 12.38 mmol) was dissolved in 50 ml of acetic acid. After addition of Rh (5% on Al2O3, 307 mg) the mixture was hydrogenated with 10 bar hydrogen and 100° C. for 120 hours. The mixture was evaporated and lyophilised. The crude material was used without purification.

Aufarbeitung

  1. customThe mixture was evaporated
  2. customThe crude material was used without purification

Quellen und Nachweise

ORD-Eintrag
ord-e9ad8eb38b184374bd02bcba4d2cf473
Quelldatensatz
uspto-grants-2006_06
Patentnummer
US07067665B2

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