Hydrochloric Acid → HCID 70274422, Verbindung

HRID 1857580Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1857580
[CH3:1][CH2:2][CH:3]([S:6]([NH2:9])(=[O:8])=[O:7])[CH2:4][CH3:5].[OH-].[Na+].[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([N:19]=[C:20]=[O:21])=[CH:15][CH:14]=1.Cl>CC(C)=O.O>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][C:20]([NH:9][S:6]([CH:3]([CH2:4][CH3:5])[CH2:2][CH3:1])(=[O:8])=[O:7])=[O:21])=[CH:15][CH:14]=1

Komponenten

7

Edukt 4

HCID 313Hydrochloric AcidHCID 76934-Chlorophenyl IsocyanateHCID 14798Sodium HydroxideHCID 22131302Pentane-3-sulfonamide

Produkt 1

HCID 70274422HCID 70274422, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 180AcetoneLösungsmittel3×HCID 962WaterLösungsmittel

Versuchsvorschrift

The general method of procedure A was followed with 3-pentanesulfonamide (10 g), acetone (300 ml), 1N sodium hydroxide (56 ml), and 4-chlorophenyl isocyanate (9.6 g) dissolved in 70 ml of acetone. After two hours of stirring, 1N HCl (66 ml) was added followed by more water. The acetone was stripped off, and the resulting solid collected, to give, after drying at 65° C. under vacuum, 13.1 g of product.

Aufarbeitung

  1. customthe resulting solid collected
  2. customto give
  3. dry with materialafter drying at 65° C. under vacuum, 13.1 g of product

Quellen und Nachweise

ORD-Eintrag
ord-6a094da47c8342ec8ab7da94d80b7250
Quelldatensatz
uspto-grants-2000_11
Patentnummer
US06147115

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