Iodoethane → HCID 178477478, Verbindung

Reaktionsgleichung

[CH3:1][O:2][C:3](=[O:24])[CH:4]([C:14]1[CH:19]=[CH:18][C:17]([NH:20][C:21]([NH2:23])=[S:22])=[CH:16][CH:15]=1)[CH2:5][NH:6][C:7]([O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8].[CH2:25](I)[CH3:26]>>[CH3:1][O:2][C:3](=[O:24])[CH:4]([C:14]1[CH:15]=[CH:16][C:17]([NH:20][C:21](=[NH:23])[S:22][CH2:25][CH3:26])=[CH:18][CH:19]=1)[CH2:5][NH:6][C:7]([O:9][C:10]([CH3:13])([CH3:12])[CH3:11])=[O:8]

Komponenten

Edukt 2

HCID 6340Iodoethane

HCID 22980982HCID 22980982, Verbindung

Produkt 1

HCID 178477478HCID 178477478, VerbindungAusbeute 96 %

Versuchsvorschrift

Using the compound obtained in Example 224 as a starting material and also using ethyl iodide as a reagent, the same procedure of Example 29 gave 0.55 g of the titled compound (yield, 96%).

Quellen und Nachweise

ORD-Eintrag: ord-d3141d4e510e450c9fbb58d385d05b4f
Quelldatensatz: uspto-grants-2003_03
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06534546B1

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