Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1865768Erstellt: 25. Oktober 2026

Methyl behenate → (2-Morpholinoethyl) behenate

https://huagongshe.com/reaction/1865768

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethyl behenateHCID 13584—
Edukt2-MorpholinoethanolHCID 61163—
KatalysatorSodium MethoxideHCID 10942334—
LösungsmittelTolueneHCID 1140—
Produkt(2-Morpholinoethyl) behenateHCID 6670541791%

Reaktionsschritte

A mixture of 35.5 g of methyl behenate (18), 19.7 g of 2-morpholinoethanol (17), 270 mg of sodium methoxide and 150 g of toluene was heated under reflux for 6 hours while distilling off the methanol resulting from the reaction. The reaction solution was cooled. By standard aqueous work-up and distilling off toluene, 41.3 g of (2-morpholinoethyl) behenate (Quencher 2) was obtained (yield 91%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07629108B2
Quelldatensatzuspto-grants-2009_12
ORD IDord-a386f213e6bd46459c2ea17f0bb9ba1b
Quellennotizuspto-grants-2009_12