HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3,4-Dichlorocinnamic acid → (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-3-methyl-[1,4]diazepan-5-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3,4-Dichlorocinnamic acid | HCID 688027 | — |
| Edukt | 3-Methyl-1,4-diazepan-5-one | HCID 68434036 | — |
| Produkt | (Rac)-1-[(e)-3-(3,4-dichloro-phenyl)-acryloyl]-3-methyl-[1,4]diazepan-5-one | HCID 68435157 | — |
Reaktionsschritte
In analogy to the procedure described in intermediate 1A, (E)-3,4-dichlorocinnamic acid and 3-methyl-[1,4]diazepan-5-one gave the title compound as a white solid. MS: 327.2 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07632829B2 |
| Quelldatensatz | uspto-grants-2009_12 |
| ORD ID | ord-c9494c340a914e88a8a6d74f4a2e0309 |
| Quellennotiz | uspto-grants-2009_12 |