HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzoic Acid → 2-Ethylhexyl benzoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzoic Acid | HCID 243 | — |
| Edukt | 2-Ethylhexanol | HCID 7720 | — |
| Katalysator | Titanium tetrabutoxide | HCID 21801 | — |
| Produkt | 2-Ethylhexyl benzoate | HCID 94310 | — |
Reaktionsschritte
In analogy to the procedure carried out in example 1, 12 mol of 2-ethylhexanol were reacted with 8 mol of benzoic acid and tetrabutyl titanate. Distillation (3 mbar, overhead temperature 134° C.) gives 2-ethylhexyl benzoate in a purity, determined by gas chromatography, of 99.7%.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07638568B2 |
| Quelldatensatz | uspto-grants-2009_12 |
| ORD ID | ord-332fb496a06f4528acc799a76d7eae9b |
| Quellennotiz | uspto-grants-2009_12 |