Ethanol → 4-(4-(Pyridin-3-yl)-1H-imidazol-1-yl)butan-1-amine

HRID 1871036Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1871036
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2[N:8]=[CH:9][N:10]([CH:12](CC)[CH2:13]N3C(=O)C4C(=CC=CC=4)C3=O)[CH:11]=2)[CH:2]=1.O.[NH2:28]N.[CH2:30](O)[CH3:31]>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2[N:8]=[CH:9][N:10]([CH2:12][CH2:13][CH2:30][CH2:31][NH2:28])[CH:11]=2)[CH:2]=1

Komponenten

4

Edukt 3

HCID 702EthanolHCID 24654Hydrazine hydrate (1:1)HCID 186948072-(4-(3-pyridinyl)-1H-imidazol-1-yl)-butyl-1H-iso-indol-1,3(2H)-dione

Produkt 1

HCID 110421604-(4-(Pyridin-3-yl)-1H-imidazol-1-yl)butan-1-amine

Versuchsvorschrift

Using the procedure of Stage B of Example 1, 1.66 g of the product of Stage A and 0.46 ml of hydrazine hydrate in 30 ml of ethanol were reacted to obtain 936 mg of the desired product which was used as is for the synthesis.

Aufarbeitung

  1. customwere reacted

Quellen und Nachweise

ORD-Eintrag
ord-bbe848dded124a9bb9282cb9a3de561e
Quelldatensatz
uspto-grants-2000_08
Patentnummer
US06100404

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