4-Chlorobenzaldehyde → E-4-chlorostyryl 4-chlorobenzyl sulfone
Reaktionsgleichung
[Cl:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7]([CH2:10][C:11](O)=O)(=[O:9])=[O:8])=[CH:4][CH:3]=1.[Cl:16][C:17]1[CH:24]=[CH:23][C:20](C=O)=[CH:19][CH:18]=1>>[Cl:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7](/[CH:10]=[CH:11]/[C:20]2[CH:23]=[CH:24][C:17]([Cl:16])=[CH:18][CH:19]=2)(=[O:9])=[O:8])=[CH:4][CH:3]=1Komponenten
3
Versuchsvorschrift
A solution of 4-chlorobenzyl sulfonylacetic acid (0.01 mol) and 4-chlorobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 80% yield.
Quellen und Nachweise
- ORD-Eintrag
- ord-608a425479bc4c6b818b22e8dd6f9303
- Quelldatensatz
- uspto-grants-2004_07
- Patentnummer
- US06767926B1
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