Hydrochloric Acid → Hydroxylauric Acid

HRID 1902398

Reaktionsgleichung

Reaktionsgleichung von HRID 1902398
Cl[CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4].[OH-:16].[K+].Cl>O>[OH:16][CH:2]([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])[C:3]([OH:5])=[O:4]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 43873702-chlorododecanoic Acid

Produkt 1

HCID 97783Hydroxylauric Acid

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

0.1 Mole of alpha-chlorolauric acid prepared in the foregoing manner was admixed with 500 mls. water and 0.4 moles of KOH in a suitable reaction vessel and stirred overnight at a temperature of 98°-100° C. The reaction mixture was poured into a separatory funnel, to which was added hydrochloric acid (40 ml. conc. HCl in 200 ml. H2O). The mixture was extracted with chloroform. The chloroform layer was removed and the CHCl3 evaporated to yield alpha-hydroxylauric acid.

Aufarbeitung

  1. additionThe reaction mixture was poured into a separatory funnel, to which
  2. extractionThe mixture was extracted with chloroform
  3. customThe chloroform layer was removed
  4. customthe CHCl3 evaporated

Quellen und Nachweise

ORD-Eintrag
ord-9737ada584704b44899546ddc2bdd5e1
Quelldatensatz
uspto-grants-1982_12
Patentnummer
US04363763

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