Hydrochloric Acid → HCID 20278358, Verbindung

HRID 1902983Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1902983
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[S:7]([NH2:10])(=[O:9])=[O:8].[CH3:11][O:12][C:13]1[N:18]=[C:17]([O:19][CH3:20])[N:16]=[C:15]([N:21]=[C:22]=[S:23])[N:14]=1.C(=O)([O-])[O-].[K+].[K+].Cl>CC(C)=O.O>[CH3:11][O:12][C:13]1[N:18]=[C:17]([O:19][CH3:20])[N:16]=[C:15]([NH:21][C:22](=[S:23])[NH:10][S:7]([C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=2)(=[O:9])=[O:8])[N:14]=1

Komponenten

7

Edukt 4

HCID 313Hydrochloric AcidHCID 11430Potassium CarbonateHCID 12000791Pyridine sulfonamideHCID 139205502-Isothiocyanato-4,6-dimethoxy-1,3,5-triazine

Produkt 1

HCID 20278358HCID 20278358, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 180AcetoneLösungsmittelHCID 962WaterLösungsmittel

Versuchsvorschrift

A mixture of 1.58 g of 2-pyridinesulfonamide, 2.04 g of 4,6-dimethoxy-2-isothiocyanato-1,3,5-triazine and 1.5 g of anhydrous potassium carbonate is stirred in 75 ml of acetone for 60 hours at ambient temperature. The reaction mixture is then poured into 500 ml of cold water, acidified with hydrochloric acid and the precipitated product removed by filtration.

Aufarbeitung

  1. customthe precipitated product removed by filtration

Quellen und Nachweise

ORD-Eintrag
ord-ce2504a0ac6145f9b10f44bf678fec11
Quelldatensatz
uspto-grants-1984_03
Patentnummer
US04435206

Notizen zur Reaktion

Wird geladen…