HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hexyl carbamate → Dihexyl carbonate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hexyl carbamate | HCID 75026 | — |
| Katalysator | zinc II acetate | HCID 131713426 | — |
| Produkt | Dihexyl carbonate | HCID 522576 | 93,9% |
Reaktionsschritte
The procedure described in Example 11 is followed, but additionally 0.5 part of zinc-II acetate is included in the reaction mixture. Analysis by gas chromatography shows that within the same period of time 94% of the n-hexyl carbamate are converted and 20.3 parts of di-n-hexyl carbonate (93.9% of theory, based on converted n-hexyl carbamate), of boiling point 122°-124° C./4 mbar have been formed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04436668 |
| Quelldatensatz | uspto-grants-1984_03 |
| ORD ID | ord-e48fef429dfc4481bdcb19bba357884e |
| Quellennotiz | uspto-grants-1984_03 |