Benzoyl Peroxide → HCID 23438954, Verbindung

HRID 1903711Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1903711
[CH3:1][C:2]1[S:3][C:4]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)=[CH:5][CH:6]=1.[Br:13]N1C(=O)CCC1=O.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>C(Cl)(Cl)(Cl)Cl>[Br:13][CH2:1][C:2]1[S:3][C:4]([C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][CH:12]=2)=[CH:5][CH:6]=1

Komponenten

5

Edukt 3

HCID 7187Benzoyl PeroxideHCID 67184N-bromobutanimideHCID 75788052-methyl-5-phenylthiophene

Produkt 1

HCID 23438954HCID 23438954, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 5943Carbon TetrachlorideLösungsmittel

Versuchsvorschrift

To a boiling solution of 2-methyl-5-phenylthiophene (2g) in dry CCl4 (100 ml) was rapidly added N-bromosuccinimide (1.94 g) and dibenzoylperoxide (0.15 g). After heating under reflux for 30 min., the mixture was cooled and filtered. Evaporation in vacuo gave the title compound as an oil (1.5 g).

Aufarbeitung

  1. temperatureAfter heating
  2. temperatureunder reflux for 30 min.
  3. temperaturethe mixture was cooled
  4. filtrationfiltered
  5. customEvaporation in vacuo

Quellen und Nachweise

ORD-Eintrag
ord-0902d85f48444f24ad68a2af63c4a5d5
Quelldatensatz
uspto-grants-1984_03
Patentnummer
US04438111

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