HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
(2S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(4-hydroxyphenyl)propanoic acid → Tyrosine Valine diaminoethane propionyl-maleimide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | (2S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(4-hydroxyphenyl)propanoic acid | HCID 6957986 | — |
| Edukt | Asparagine Valine diaminoethane propionyl-maleimide | HCID 131731084 | — |
| Produkt | Tyrosine Valine diaminoethane propionyl-maleimide | HCID 131731083 | — |
Reaktionsschritte
AF-Tyrosine-Valine-diaminoethane-propionyl-maleimide (5d) was prepared in the same manner as 5c, using Fmoc-Tyr for AA1. Yield: 36 mg (68%) of white solid. RP-HPLC analysis: >95% at 7.8 min; ESMS m/z=1201.67 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08609105B2 |
| Quelldatensatz | uspto-grants-2013_12 |
| ORD ID | ord-f08853bc42d44319ad12d365d6998f20 |
| Quellennotiz | uspto-grants-2013_12 |