Hydroxylamine → 5-(5-Ethyl-2-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-furan-2-carbaldehyde oxime

HRID 1921474Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1921474
[CH2:1]([C:3]1[C:8](=[O:9])[NH:7][C:6]([CH3:10])=[C:5]([C:11]2[O:15][C:14]([CH:16]=O)=[CH:13][CH:12]=2)[CH:4]=1)[CH3:2].[NH2:18][OH:19]>>[CH2:1]([C:3]1[C:8](=[O:9])[NH:7][C:6]([CH3:10])=[C:5]([C:11]2[O:15][C:14]([CH:16]=[N:18][OH:19])=[CH:13][CH:12]=2)[CH:4]=1)[CH3:2]

Komponenten

3

Edukt 2

HCID 787HydroxylamineHCID 588086555-(5-Ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl)furan-2-carbaldehyde

Produkt 1

HCID 1364153265-(5-Ethyl-2-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-furan-2-carbaldehyde oxime

Versuchsvorschrift

Example 198 is substantially repeated except for utilizing 5-(5-ethyl-2-methyl-6-oxo-1,6-dihydropyridin-3-yl]furan-2-carbaldehyde and hydroxylamine to afford the title compound. MS: m/e=247 (M+H).

Quellen und Nachweise

ORD-Eintrag
ord-802cd1148e77421e9057d29d93ff84d1
Quelldatensatz
uspto-grants-2012_05
Patentnummer
US08173682B2

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