3-Nitro-N-(pyridin-4-yl)pyridin-2-amine → HCID 12445535, Verbindung

HRID 1974324Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1974324
[N+:1]([C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1)([O-])=O>[Pd].CO>[NH2:1][C:4]1[C:5]([NH:10][C:11]2[CH:16]=[CH:15][N:14]=[CH:13][CH:12]=2)=[N:6][CH:7]=[CH:8][CH:9]=1

Komponenten

4

Edukt 1

HCID 124453923-Nitro-N-(pyridin-4-yl)pyridin-2-amine

Produkt 1

HCID 12445535HCID 12445535, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 2

HCID 23938PalladiumKatalysatorHCID 887MethanolLösungsmittel

Versuchsvorschrift

The nitro compound from Step A (1.0 g.) was hydrogenated in 60 ml. of methanol over 0.2 g. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the filtrate was evaporated to dryness.

Aufarbeitung

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated to dryness

Quellen und Nachweise

ORD-Eintrag
ord-ea124cf1a6c54326bf7e664de0c6bc0c
Quelldatensatz
uspto-grants-1976_12
Patentnummer
US04000286

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