Ammonium Hydroxide → HCID 66958625, Verbindung
Reaktionsgleichung
[CH2:1]([N:3]1[C:7]([CH2:8][CH2:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:6][C:5]([C:14]([O:16]CC)=O)=[N:4]1)[CH3:2].[OH-].[NH4+:20]>>[CH2:1]([N:3]1[C:7]([CH2:8][CH2:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:6][C:5]([C:14]([NH2:20])=[O:16])=[N:4]1)[CH3:2]Komponenten
3
Versuchsvorschrift
The method described in Part C of Example 10 was used to treat ethyl 1-ethyl-5-(2-methanesulfonylethyl)-1H-pyrazole-3-carboxylate (4.6 g, 17 mmol) with ammonium hydroxide (100 mL). The solid was isolated by filtration and washed with water to provide 3.0 g of 1-ethyl-5-(2-methanesulfonylethyl)-1H-pyrazole-3-carboxamide as a white powder, which was mixed with material from another run.
Aufarbeitung
- customThe solid was isolated by filtration
- washwashed with water
Quellen und Nachweise
- ORD-Eintrag
- ord-70cdd03781574f679e9617e0ffd1bfb6