Hydrochloric Acid → methyl 1H-tetrazol-1-ylacetate

HRID 20268Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 20268
[N:1]1([CH2:6][C:7]([OH:9])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1.Cl.O1CCOC[CH2:12]1>CO>[N:1]1([CH2:6][C:7]([O:9][CH3:12])=[O:8])[CH:5]=[N:4][N:3]=[N:2]1

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 312751,4-DioxaneHCID 5432071-Tetrazolylacetic acid

Produkt 1

HCID 3153776methyl 1H-tetrazol-1-ylacetate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

A mixture of tetrazol-1-yl acetic acid (5 g, 39 mmol) and 4M hydrochloric acid in dioxan (100 μL) in methanol (50 mL) was heated under reflux for 18 hours. The cooled mixture was evaporated under reduced pressure to provide the title compound.

Aufarbeitung

  1. temperaturewas heated
  2. temperatureunder reflux for 18 hours
  3. customThe cooled mixture was evaporated under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-2eec8cc3221c4243826d62a42e0801a2
Quelldatensatz
uspto-grants-2010_06
Patentnummer
US07745630B2

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