Sodium Carbonate Decahydrate → Pentabromodiphenyl ethers

HRID 2058053

Reaktionsgleichung

Reaktionsgleichung von HRID 2058053
[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1.P(OC1C=CC=CC=1)(OC1C=CC=CC=1)(OCC(CC)CCCC)=O.O.O.O.O.O.O.O.O.O.O.C(=O)([O-])[O-].[Na+].[Na+]>O>[CH:1]1[C:6]([Br:7])=[CH:5][C:4]([Br:8])=[C:3]([O:9][C:10]2[C:15]([Br:16])=[CH:14][C:13]([Br:17])=[C:12]([Br:18])[CH:11]=2)[CH:2]=1

Komponenten

4

Edukt 2

HCID 151402Sodium Carbonate DecahydrateHCID 131711832HCID 131711832, Verbindung

Produkt 1

HCID 36159Pentabromodiphenyl ethers

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Using the procedure of Examples II and IV, the pentabromodiphenyl ether-2-ethylhexyl diphenyl phosphate blend was heated to 130° C., and sodium carbonate decahydrate (2.7% W/W on the blend) was added and subjected to agitation in the closed system for one-half hour. Thereafter, the system was opened in order to permit water to escape. The molten mixture was filtered to obtain the purified blend. Relevant properties of the blend are given in Table III.

Aufarbeitung

  1. waitsubjected to agitation in the closed system for one-half hour
  2. filtrationThe molten mixture was filtered
  3. customto obtain the purified blend

Quellen und Nachweise

ORD-Eintrag
ord-e3755f6f64ff4cec9d58fbca0c3ac339
Quelldatensatz
uspto-grants-1980_07
Patentnummer
US04214103

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