HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Succinic Acid → 1-Cyclooctylmethylimidazole hydrogen succinate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Succinic Acid | HCID 1110 | — |
| Edukt | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-Cyclooctylmethylimidazole hydrogen succinate | HCID 20550250 | 44,7% |
Reaktionsschritte
A solution of succinic acid (0.23 g) in ethanol (~5 ml) was added to a solution of 1-cyclooctylmethylimidazole (0.38 g) in ethanol (5 ml). Evaporation of the solution afforded a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen succinate (0.27 g) as colourless plates, m.p. 86° to 87° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04317830 |
| Quelldatensatz | uspto-grants-1982_03 |
| ORD ID | ord-f3c8a4fd58044f61b41eedb23a9e3b99 |
| Quellennotiz | uspto-grants-1982_03 |