HRID2058448

反应详情

EQUATION

反应方程式

HRID 2058448 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of succinic acid (0.23 g) in ethanol (~5 ml) was added to a solution of 1-cyclooctylmethylimidazole (0.38 g) in ethanol (5 ml). Evaporation of the solution afforded a white solid. Recrystallisation of the solid from ethyl acetate afforded 1-cyclooctylmethylimidazole hydrogen succinate (0.27 g) as colourless plates, m.p. 86° to 87° C.

WORKUP

后处理

  1. customEvaporation of the solution
  2. customafforded a white solid
  3. customRecrystallisation of the solid from ethyl acetate