HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 1-Cyclooctylmethylimidazole hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | 1-Cyclooctylmethylimidazole hydrochloride | HCID 20550255 | — |
Reaktionsschritte
1-Cyclooctylmethylimidazole (~0.3 g) was dissolved in dry ether (30 ml), when a stream of dry hydrogen chloride was passed through the solution at -20° C. The resulting white precipitate was filtered off under dry nitrogen and recrystallised from ethyl acetate/petroleum ether (b.p. 40°-60° C.) to afford 1-cyclooctylmethylimidazole hydrochloride as a white solid, m.p. 20°-22° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04317830 |
| Quelldatensatz | uspto-grants-1982_03 |
| ORD ID | ord-5bdd3835cb974ba2bc4d7b9ee7b35fb0 |
| Quellennotiz | uspto-grants-1982_03 |