Piperonal → Ilepcimide
Reaktionsgleichung
O=Cc1ccc2c(c1)OCO2.O=C(O)CC(=O)N1CCCCC1>NCc1ccccc1.O=C(O)C(F)(F)F.CN(C)c1ccncc1.CN(C)C=O>O=C(/C=C/c1ccc2c(c1)OCO2)N1CCCCC1Komponenten
6
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 3
Reaktionsbedingungen
- Temperatur
- 50 °C
Aufarbeitung
- temperatureThe product mixture was cooled to 25 °C.
- filtrationFiltered through a pad of celite · Organic-Phase beibehalten
- wash"The celite was washed with ethyl acetate (3 x 1 mL)."
- concentrationThe filtrate was concentrated under reduced pressure
- additionA 0.07 M stock solution of the internal standard ethylene carbonate (0.70 mL in CDCl3) was added.
Quellen und Nachweise
- ORD-Eintrag
- ord-fbf96c68eb8d41da8e80972be2e70ec1
- Quelldatensatz
- Transfer learning optimization of 26 decarboxylative olefination reactions
Notizen zur Reaktion
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