HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Bromobenzyl bromide → 1-Bromo-4-((methylsulfonyl)methyl)benzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Bromobenzyl bromide | HCID 68527 | — |
| Edukt | HCID 178504973 | HCID 178504973 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | 1-Bromo-4-((methylsulfonyl)methyl)benzene | HCID 2761415 | — |
Reaktionsschritte
p-Bromobenzyl bromide (500 mg, 2 mmol) was refluxed with MeSO2Na (306 mg, 3 mmol) in Ethanol for 1 hour. The reaction was cooled, concentrated and purified by flash column (50% acetone/hexanes) to give the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08445499B2 |
| Quelldatensatz | uspto-grants-2013_05 |
| ORD ID | ord-eda08050a15f4ecd80044bec3b2dae57 |
| Quellennotiz | uspto-grants-2013_05 |