HRID2093485

反应详情

EQUATION

反应方程式

HRID 2093485 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

p-Bromobenzyl bromide (500 mg, 2 mmol) was refluxed with MeSO2Na (306 mg, 3 mmol) in Ethanol for 1 hour. The reaction was cooled, concentrated and purified by flash column (50% acetone/hexanes) to give the desired product.

WORKUP

后处理

  1. temperatureThe reaction was cooled
  2. concentrationconcentrated
  3. custompurified by flash column (50% acetone/hexanes)