2-Methoxyethylamine → N-(2-methoxyethyl)methanesulfonamide
Reaktionsgleichung
[CH3:1][O:2][CH2:3][CH2:4][NH2:5].C(N(CC)CC)C.[CH3:13][S:14](Cl)(=[O:16])=[O:15]>ClCCl>[CH3:1][O:2][CH2:3][CH2:4][NH:5][S:14]([CH3:13])(=[O:16])=[O:15]Komponenten
5
Edukt 3
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
To a stirring solution of 2-methoxyethylamine (0.58 ml) in dichloromethane (10 ml) was added triethylamine (1.0 ml) and methanesulphonyl chloride (0.51 ml). The mixture was stirred at room temperature overnight. The solvents were removed in vacuo to give a crude product which was purified by flash chromatography to give N-(2-Methoxy-ethyl)-methanesulfonamide (0.74 g).
Aufarbeitung
- customThe solvents were removed in vacuo
- customto give a crude product which
- customwas purified by flash chromatography
Quellen und Nachweise
- ORD-Eintrag
- ord-5c533c63910049a7973a3ff144baf9cf
- Quelldatensatz
- uspto-grants-2013_05
- Patentnummer
- US08450315B2
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