1-Chloro-2-(diethylamine)ethane hydrochloride → HCID 69065330, Verbindung

HRID 2109022Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2109022
[C:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11]([OH:13])=[O:12])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[OH-].[Na+].[CH3:16][CH2:17][N:18]([CH2:21][CH2:22]Cl)[CH2:19][CH3:20].Cl>O>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([S:11]([CH2:16][CH2:17][N:18]([CH2:21][CH3:22])[CH2:19][CH3:20])(=[O:13])=[O:12])=[CH:9][CH:10]=1)(=[O:3])[CH3:2]

Komponenten

5

Edukt 3

HCID 133631-Chloro-2-(diethylamine)ethane hydrochlorideHCID 14798Sodium Hydroxide2×HCID 4121504-(Acetylamino)benzenesulfinic acid

Produkt 1

HCID 69065330HCID 69065330, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

9.0 g of 4-acetamido-phenylsulphinic acid are dissolved in 10 ml of water and 45 ml of 1N sodium hydroxide solution and 9.47 g of 2-chlorotriethylamine hydrochloride are added. The mixture is stirred for 5 hours at reflux temperature. After cooling, sodium hydroxide solution is added until an alkaline reaction is obtained, the mixture is extracted with ethyl acetate, dried over magnesium sulphate and finally the solvent is eliminated.

Aufarbeitung

  1. temperatureat reflux temperature
  2. temperatureAfter cooling
  3. customis obtained
  4. extractionthe mixture is extracted with ethyl acetate
  5. dry with materialdried over magnesium sulphate

Quellen und Nachweise

ORD-Eintrag
ord-d6396b351f864c0abea1e4bff9a0de9c
Quelldatensatz
uspto-grants-2009_04
Patentnummer
US07514468B2

Notizen zur Reaktion

Wird geladen…