Hydrochloric Acid → 5,6-Indandicarboxylic acid
Reaktionsgleichung
[CH2:1]1[C:9]2[C:4](=[CH:5][C:6]([C:15]([O:17]CC)=[O:16])=[C:7]([C:10]([O:12]CC)=[O:11])[CH:8]=2)[CH2:3][CH2:2]1.Cl>C(O)(=O)C>[CH2:1]1[C:9]2[C:4](=[CH:5][C:6]([C:15]([OH:17])=[O:16])=[C:7]([C:10]([OH:12])=[O:11])[CH:8]=2)[CH2:3][CH2:2]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 80 °C
Versuchsvorschrift
To a solution of the product of above-mentioned (a) (0.36 g, 1.4 mmol) in acetic acid (0.8 ml) was added concentrated hydrochloric acid (0.4 ml) and stirred at 80° C. overnight. To the reaction solution was added ice-cold water, and the precipitated crystals were collected by filtration, washed with water, followed by drying to give 0.28 g of 5,6-indandicarboxylic acid.