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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2118488Erstellt: 25. Oktober 2026

1-Phenylpiperazine → 7-[4-(4-Phenyl-1-piperazinyl)butoxy]-4H-1-benzopyran-4-one

https://huagongshe.com/reaction/2118488

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt1-PhenylpiperazineHCID 7096—
Edukt7-(4-Chlorobutoxy)-4H-1-benzopyran-4-oneHCID 13923967—
LösungsmittelWaterHCID 962—
Produkt7-[4-(4-Phenyl-1-piperazinyl)butoxy]-4H-1-benzopyran-4-oneHCID 13923985—

Reaktionsschritte

The title compound was prepared by the method described above in Examples 1-3. Thus, 7-(4-chlorobutoxy)-4H-1-benzopyran-4-one, as prepared above in Preparation 2, (3.79 g, 15 mmol) was treated with 1-phenylpiperazine (2.59 g; 16 mmol) in the usual way, yielding 3.76 g of 7-[4-(4-phenyl-1-piperazinyl)butoxy-]4H-1-benzopan-4-one.1.5 HCL (H2O), mp 204°-206° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04678787
Quelldatensatzuspto-grants-1987_07
ORD IDord-a85370b7c7b14e52b8e297db2b345759
Quellennotizuspto-grants-1987_07