Formic Acid → 3-Butyl-6-formamido-phthalide

HRID 2120180

Reaktionsgleichung

Reaktionsgleichung von HRID 2120180
[NH2:1][C:2]1[CH:11]=[C:10]2[C:5]([CH:6]([CH2:12][CH2:13][CH2:14][CH3:15])[O:7][C:8]2=[O:9])=[CH:4][CH:3]=1.[CH:16](O)=[O:17]>>[CH2:12]([CH:6]1[C:5]2[C:10](=[CH:11][C:2]([NH:1][CH:16]=[O:17])=[CH:3][CH:4]=2)[C:8](=[O:9])[O:7]1)[CH2:13][CH2:14][CH3:15]

Komponenten

3

Edukt 2

HCID 284Formic AcidHCID 98777066-Amino-3-butyl-phthalide

Produkt 1

HCID 98345703-Butyl-6-formamido-phthalide

Versuchsvorschrift

A solution of 3.07 g (0.015 mol) of the compound obtained in Example 4 in 15 ml of 85% formic acid is heated to 60° C. An hour later the reaction mixture is poured into ice-water. The separated solid is collected and crystallised from dilute ethanol to give the title compound.

Aufarbeitung

  1. customThe separated solid is collected
  2. customcrystallised from dilute ethanol

Quellen und Nachweise

ORD-Eintrag
ord-3ff838d2a1064b6aa58b0000a78b057b
Quelldatensatz
uspto-grants-2004_02
Patentnummer
US06689808B2

Verknüpfte Notizen

Wird geladen…