Hydrogen Bromide → 2-Bromomethyl-6-methyl benzoic acid

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Reaktionsgleichung

[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]([CH3:11])[C:3]=1[C:4]([OH:6])=[O:5].[Br:12]([O-])(=O)=O.[Na+].Br>>[Br:12][CH2:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]([CH3:11])[C:3]=1[C:4]([OH:6])=[O:5]

Komponenten

Edukt 3

HCID 260Hydrogen Bromide

HCID 124392,6-Dimethylbenzoic acid

HCID 23668195Sodium Bromate

Produkt 1

HCID 99913982-Bromomethyl-6-methyl benzoic acid

Versuchsvorschrift

It has now been found that the reaction of 2,6-dimethyl-benzoic acid (II) with sodium bromate and hydrobromic acid in the presence of light gives 2-bromomethyl-6-methyl benzoic acid (I) in high yield and purity.

Quellen und Nachweise

ORD-Eintrag: ord-f76935f6242b44928ca7abdc57d1cf6d
Quelldatensatz: uspto-grants-2004_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06689891B2

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