HCID 178420353, Verbindung → HCID 178511580, Verbindung
Reaktionsgleichung
C([N:8](CC1C=CC=CC=1)[C@H:9]1[CH2:14][CH2:13][C@H:12]([N:15]2[CH2:20][CH2:19][O:18][CH2:17][CH2:16]2)[CH2:11][CH2:10]1)C1C=CC=CC=1>CO.[Pd]>[O:18]1[CH2:17][CH2:16][N:15]([C@H:12]2[CH2:11][CH2:10][C@H:9]([NH2:8])[CH2:14][CH2:13]2)[CH2:20][CH2:19]1Komponenten
4
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
7.2 g (16.4 mmol) trans-dibenzyl-4-morpholino-cyclohexylamine were dissolved in 100 mL methanol and hydrogenated on 1.4 g Pd/C (10%) at 30-50° C. The solvent was eliminated in vacuo and the residue was crystallised from ethanol and conc. hydrochloric acid.
Aufarbeitung
- customthe residue was crystallised from ethanol and conc. hydrochloric acid
Quellen und Nachweise
- ORD-Eintrag
- ord-81562d501d5a4d39a2ba2aae8b24ade3
- Quelldatensatz
- uspto-grants-2012_06
- Patentnummer
- US08193188B2
Notizen zur Reaktion
Wird geladen…