HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Anhydride → Citronellyl Acetate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Anhydride | HCID 7918 | — |
| Edukt | Citronellol | HCID 8842 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | Citronellyl Acetate | HCID 9017 | — |
Reaktionsschritte
100 Grams of 3,7-dimethyloct-6-en-1-ol is dissolved in 150 ml. of pyridine and 100 ml. of acetic anhydride and left at room temperature for about 48 hours. Then the mixture is extracted with ether and the ethereal extracts washed with water, 10% aqueous HCl and brine to yield 1-acetoxy-3,7-dimethyloct-6-ene which is purified by distillation.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04137273 |
| Quelldatensatz | uspto-grants-1979_01 |
| ORD ID | ord-bd39ca3e5fdc410baafd6f53f8e929f7 |
| Quellennotiz | uspto-grants-1979_01 |