HRID2164189

反应详情

EQUATION

反应方程式

HRID 2164189 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

100 Grams of 3,7-dimethyloct-6-en-1-ol is dissolved in 150 ml. of pyridine and 100 ml. of acetic anhydride and left at room temperature for about 48 hours. Then the mixture is extracted with ether and the ethereal extracts washed with water, 10% aqueous HCl and brine to yield 1-acetoxy-3,7-dimethyloct-6-ene which is purified by distillation.

WORKUP

后处理

  1. extractionThen the mixture is extracted with ether
  2. washthe ethereal extracts washed with water, 10% aqueous HCl and brine