Acetic Acid → Cadmium acetate

Reaktionsgleichung

[F-].[Cd+2:2].[F-].[Cd].OO.[C:7]([OH:10])(=[O:9])[CH3:8]>>[C:7]([O-:10])(=[O:9])[CH3:8].[Cd+2:2].[C:7]([O-:10])(=[O:9])[CH3:8]

Komponenten

Edukt 4

HCID 176Acetic Acid

HCID 784Hydrogen Peroxide

HCID 23973Cadmium

HCID 10130045Cadmium fluoride [MI]

Produkt 1

HCID 10986Cadmium acetate

Versuchsvorschrift

The preparation procedure for cadmium fluoride is somewhat different. High purity cadmium metal (typically 99.999 percent pure) is reacted with acetic acid and hydrogen peroxide to yield cadmium acetate. This compound is then reacted with hydrogen fluoride to yield cadmium fluoride. The cadmium fluoride is slowly heated to the melting point in an atmosphere of carbon tetrafluoride to ensure removal of water, oxide and oxyfluoride.