3,5-Dimethyl-4-nitrocyclohex-1-ene → 2,6-Dimethylcyclohexylamine

HRID 2164687Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2164687
[CH3:1][CH:2]1[CH:7]([N+:8]([O-])=O)[CH:6]([CH3:11])[CH2:5][CH:4]=[CH:3]1.[H][H]>[Pd]>[CH3:11][CH:6]1[CH2:5][CH2:4][CH2:3][CH:2]([CH3:1])[CH:7]1[NH2:8]

Komponenten

4

Edukt 2

HCID 204053483,5-Dimethyl-4-nitrocyclohex-1-eneHCID 178418361HCID 178418361, Verbindung

Produkt 1

HCID 1109322,6-Dimethylcyclohexylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 23938PalladiumKatalysator

Versuchsvorschrift

contacting said 3,5-dimethyl-4-nitro-cyclohexene with hydrogen at a temperature of about 0° C. to about 200° C. and a pressure of about 0 psig to about 1500 psig in the presence of a palladium catalyst to form 2,6-dimethylcyclohexyl amine; and

Aufarbeitung

  1. customat a temperature of about 0° C. to about 200° C.

Quellen und Nachweise

ORD-Eintrag
ord-cdaada7ceb2a4cfe80bb83c656bd31ab
Quelldatensatz
uspto-grants-1985_03
Patentnummer
US04506098

Notizen zur Reaktion

Wird geladen…