Reaktionsgleichung
O[CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9].[CH2:10]([SH:12])[CH3:11]>>[CH2:10]([S:12][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[OH:9])[CH3:11]Komponenten
3
Versuchsvorschrift
A mixture of 49.6 g (0.4 mol) of 2-hydroxymethyl-phenol and 124 g (2 mol) of ethylmercaptan was heated for 5 hours to 170° C. in a stirred autoclave. Working up as in Example 1 gave 32.2 g (96% of theory) of 2-ethylthiomethyl-phenol.
Aufarbeitung
- temperaturewas heated for 5 hours to 170° C. in a stirred autoclave
Quellen und Nachweise
- ORD-Eintrag
- ord-eacb17e009e84059b307f1326fc1641a
- Quelldatensatz
- uspto-grants-1982_11
- Patentnummer
- US04358616
Verknüpfte Notizen
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