2-Bromopropane → HCID 20519071, Verbindung

HRID 2198798

Reaktionsgleichung

Reaktionsgleichung von HRID 2198798
[OH:1][CH2:2][CH:3]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4]1.Br[CH:16]([CH3:18])[CH3:17]>O>[CH:3]1([CH2:2][O:1][CH:16]([CH3:18])[CH3:17])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1

Komponenten

4

Edukt 2

HCID 63582-BromopropaneHCID 74686Cyclododecanemethanol

Produkt 1

HCID 20519071HCID 20519071, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

According to the disclosure of Example 1, 99 g of hydroxymethylcyclododecane was first converted into the sodium alcoholate. 74 g (0.6 mol) of 2-bromopropane was added dropwise to the boiling suspension, and then the mixture was heated for 30 hours under reflux. The reaction mixture was poured into water, the organic phase was washed with water, dried over Na2SO4, and then distilled.

Aufarbeitung

  1. temperaturethe mixture was heated for 30 hours
  2. temperatureunder reflux
  3. washthe organic phase was washed with water
  4. dry with materialdried over Na2SO4
  5. distillationdistilled

Quellen und Nachweise

ORD-Eintrag
ord-dcbf17b5baba4e33805706cfee481f0a
Quelldatensatz
uspto-grants-1982_11
Patentnummer
US04359588

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