Zurück
HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2216339Erstellt: 25. Oktober 2026

Hydrogen Bromide → HCID 178515992, Verbindung

https://huagongshe.com/reaction/2216339

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHydrogen BromideHCID 260—
Edukt2-Benzyl-6-methoxypyridineHCID 21942274—
LösungsmittelWaterHCID 962—
ProduktHCID 178515992HCID 17851599270,9%

Reaktionsbedingungen

Temperatur100 °C

Reaktionsschritte

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07112593B2
Quelldatensatzuspto-grants-2006_09
ORD IDord-8432c46a7bbf42feb057a7de3b73cea2
Quellennotizuspto-grants-2006_09