反应详情

温度

100 °C

A mixture of 59 g of 2-benzyl-6-methoxypyridine and 200 ml of 47% hydrobromic acid was heated under stirring in an oil bath at 100° C. for 7 hours. After standing to cool, 250 ml of water was added and the resulting crystals were filtered, washed with water and dried under reduced pressure, to give 38.9 g of the title compound.

1. temperaturewas heated
2. temperatureto cool
3. filtrationthe resulting crystals were filtered
4. washwashed with water
5. customdried under reduced pressure