Cyclobutanone → HCID 9980289, Verbindung
Reaktionsgleichung
[I:1][C:2]1[C:12]([O:13][CH2:14][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[CH:11][C:5]2[CH2:6][CH2:7][NH:8][CH2:9][CH2:10][C:4]=2[CH:3]=1.[C:21]1(=O)[CH2:24][CH2:23][CH2:22]1.C1(N2CCC3C=C(I)C(OC4N=CC(C(NC)=O)=CC=4)=CC=3CC2)CCC1>>[CH:21]1([N:8]2[CH2:7][CH2:6][C:5]3[CH:11]=[C:12]([O:13][CH2:14][C:15]4[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=4)[C:2]([I:1])=[CH:3][C:4]=3[CH2:10][CH2:9]2)[CH2:24][CH2:23][CH2:22]1Komponenten
4
Versuchsvorschrift
Example 226 (E226) was prepared from 7-iodo-8-[(phenylmethyl)oxy]-2,3,4,5-tetrahydro-1H-3-benzazepine (D45) and cyclobutanone using the method described for Example 225 (E225); MS (ES+) m/e 434 [M+H]+.