1,2-Epoxydodecane → 1-(2-Hydroxydodecyl)-2-(2-pyridyl)imidazole

HRID 223772

Reaktionsgleichung

Reaktionsgleichung von HRID 223772
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[NH:8][CH:9]=[CH:10][N:11]=1.[O:12]1[CH:14]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:13]1>O>[OH:12][CH:14]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])[CH2:13][N:11]1[CH:10]=[CH:9][N:8]=[C:7]1[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1

Komponenten

4

Edukt 2

HCID 178581,2-EpoxydodecaneHCID 5893132-(1H-imidazol-2-yl)pyridine

Produkt 1

HCID 205207621-(2-Hydroxydodecyl)-2-(2-pyridyl)imidazole

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterKatalysator

Reaktionsbedingungen

Temperatur
160 °C

Versuchsvorschrift

A mixture of 14.5 g (0.1 mole) 2-(2-pyridyl)imidazole, 18.4 g (0.1 mole) 1,2-epoxydodecane and 3 drops of water was heated with stirring at about 160° C. under nitrogen for about one hour. The resulting product was then extracted with hot hexane and collected as yellow crystals which had a melting point of 62°-65° C.

Aufarbeitung

  1. temperaturewas heated
  2. extractionThe resulting product was then extracted with hot hexane
  3. customcollected as yellow crystals which

Quellen und Nachweise

ORD-Eintrag
ord-a370c73d7c074116a7ccd29da8475232
Quelldatensatz
uspto-grants-1982_10
Patentnummer
US04356309

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