Water → N-butylprop-2-enamide;prop-2-enamide

HRID 2243780Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2243780
[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].C([C:10](=[CH2:14])[C:11]([NH2:13])=[O:12])CCC.[CH:15]([C:17]1C=CC=C[C:18]=1C=C)=[CH2:16].O>C(O)C>[C:1]([NH2:5])(=[O:4])[CH:2]=[CH2:3].[CH2:16]([NH:13][C:11](=[O:12])[CH:10]=[CH2:14])[CH2:15][CH2:17][CH3:18]

Komponenten

6

Edukt 4

HCID 962WaterHCID 6579AcrylamideHCID 666661,2-DiethenylbenzeneHCID 12525275Butylacrylamide

Produkt 1

HCID 20215358N-butylprop-2-enamide;prop-2-enamide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

Polystyrenesulfonate (22.5 mmoles, 3.918 g), acrylamide (3.45 mmoles, 0.245 g), n-butylacrylamide (3.45 mmoles, 0.439 g) and divinylbenzene (0.6 mmoles, 85.5 microL) were dissolved in 15 mL ethanol and 5 mL water in a 40 mL vial fitted with a septa cap. The solution was degassed by bubbling nitrogen through and 1 mole % AIBN was added as a solution. The polymerization solution was further degassed and the placed in a heated reaction block at 60° C. for 18 h. A clear, light yellow gel formed.

Aufarbeitung

  1. customThe solution was degassed
  2. customby bubbling nitrogen through and 1 mole % AIBN
  3. additionwas added as a solution
  4. customThe polymerization solution was further degassed
  5. customthe placed in a heated reaction block at 60° C. for 18 h
  6. customA clear, light yellow gel formed

Quellen und Nachweise

ORD-Eintrag
ord-b5e6350914224e22871e3835626e2adb
Quelldatensatz
uspto-grants-2010_03
Patentnummer
US07678369B2

Notizen zur Reaktion

Wird geladen…