Triethyl Citrate → Ethyl Acetoacetate
Reaktionsgleichung
C(OCC)(=O)[CH2:2][C:3]([CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])(C(OCC)=O)[OH:4]>CC([O-])C.CC([O-])C.CC([O-])C.CC([O-])C.[Ti+4]>[C:11]([O:13][CH2:14][CH3:15])(=[O:12])[CH2:10][C:3]([CH3:2])=[O:4]Komponenten
3
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
In the same way as in Example 1, 60 g (0.21 mol) of tetraisopropyl titanate were reacted with 116.6 g (0.42 mol) of triethyl citrate. The mixture was freed of alcohol under vacuum and 154.6 g of a clear, pale yellow liquid was obtained.
Aufarbeitung
- customwas obtained
Quellen und Nachweise
- ORD-Eintrag
- ord-0b1f2e1c0f294ff991c72bb3ca95134c
- Quelldatensatz
- uspto-grants-1995_06
- Patentnummer
- US05428103
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