Azobisisobutyronitrile → Methyl Methacrylate

HRID 224763

Reaktionsgleichung

Reaktionsgleichung von HRID 224763
[CH2:1]([N:3]([CH2:6][CH2:7][O:8][C:9](=[O:12])[CH:10]=[CH2:11])[CH2:4][CH3:5])[CH3:2].[CH2:13](OC(=O)C(C)=C)CCCCCCCCCCCCCCCCC.[CH3:37][O:38][C:39](=[O:43])[C:40]([CH3:42])=[CH2:41].CC(N=NC(C#N)(C)C)(C#N)C>C1C=CC=CC=1>[CH2:1]([N:3]([CH2:6][CH2:7][O:8][C:9](=[O:12])[C:10]([CH3:13])=[CH2:11])[CH2:4][CH3:5])[CH3:2].[CH3:37][O:38][C:39](=[O:43])[C:40]([CH3:42])=[CH2:41]

Komponenten

7

Edukt 4

HCID 6547AzobisisobutyronitrileHCID 6658Methyl MethacrylateHCID 170502-(Diethylamino)ethyl acrylateHCID 122600Stearyl methacrylate

Produkt 2

HCID 6658Methyl MethacrylateHCID 61012Diethylaminoethyl Methacrylate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 241BenzeneLösungsmittel

Versuchsvorschrift

A copolymer of 2-(N',N'-diethylamino)ethylmethacrylate, stearylmetacrylate, and methylmethacrylate was prepared by charging 0.048 mole of 2-(N',N'-diethylamino)ethylacrylate, 0.002 moles of stearylmethacrylate and 0.15 moles of methylmethacrylate in a retort containing 0.002 moles of AIBN. The retort had in accordance with Example 1 been gassed with nitrogen gas for half an hour before charging. The components were dissolved in dry benzene.

Aufarbeitung

  1. waitbeen gassed with nitrogen gas for half an hour

Quellen und Nachweise

ORD-Eintrag
ord-a8b5c3de89444517adf150eafbb00e2e
Quelldatensatz
uspto-grants-1980_11
Patentnummer
US04234565

Verknüpfte Notizen

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