HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
7-Chloro-2-methylquinoline → Dimethyl 5-(3-(2-(7-chloroquinolin-2-yl)ethenyl)phenyl)-4,6-dithianonanedioate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 7-Chloro-2-methylquinoline | HCID 138395 | — |
| Edukt | Dimethyl 3,3'-(((3-formylphenyl)methylene)bis(sulfanediyl))dipropanoate | HCID 10021188 | — |
| Lösungsmittel | Acetic Anhydride | HCID 7918 | — |
| Produkt | Dimethyl 5-(3-(2-(7-chloroquinolin-2-yl)ethenyl)phenyl)-4,6-dithianonanedioate | HCID 53731421 | — |
Reaktionsschritte
A solution of aldehyde (Step 1) (5.2 g) and 7-chloroquinaldine were heated in 45 ml acetic anhydride for 48 hours. The reaction mixture was evaporated. Flash chromatography of the residue using 5% ethylacetate in hexane afforded the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05428171 |
| Quelldatensatz | uspto-grants-1995_06 |
| ORD ID | ord-cfa2eb7e011a42859db8e0347809ca74 |
| Quellennotiz | uspto-grants-1995_06 |