HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glycidol → 1,2-Propanediol, 3-(dodecylamino)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glycidol | HCID 11164 | — |
| Edukt | Dodecylamine | HCID 13583 | — |
| Produkt | 1,2-Propanediol, 3-(dodecylamino)- | HCID 102496 | — |
Reaktionsschritte
Dodecylamine (25.02 g, 0.13 mole) was heated to 85° C. Glycidol (10 g, 0.13 mole) was added dropwise. The reaction solution was heated under nitrogen for 3 hours and was stirred overnight at room temperature. A white solid was obtained (crude yield=33.27 g). The solid was recrystalized from hot hexane (crystallized 10.86 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05476671 |
| Quelldatensatz | uspto-grants-1995_12 |
| ORD ID | ord-1154cc03e7904ae0a02dac36e85a2e70 |
| Quellennotiz | uspto-grants-1995_12 |