HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → p-Trifluoromethoxybenzaldehyde oxime
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | p-(Trifluoromethoxy)benzaldehyde | HCID 69573 | — |
| Edukt | Hydroxyamine hydrochloride | HCID 443297 | — |
| Produkt | p-Trifluoromethoxybenzaldehyde oxime | HCID 2777199 | 94% |
Reaktionsschritte
In a similar manner as described in Preparation Example 1, by using 4-(trifluoromethoxy)benzaldehyde (38.02 g, 200.0 mmol), sodium hydroxide (12.00 g, 300.0 mmol) and hydrochloric acid hydroxylamine (16.68 g, 240 mmol), a white solid required compound (38.68 g, 188 mmol, 94%) was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09132126B2 |
| Quelldatensatz | uspto-grants-2015_09 |
| ORD ID | ord-2d1b21b657f145ceb454501707d3938c |
| Quellennotiz | uspto-grants-2015_09 |