Hydrochloric Acid → 1,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

HRID 2290601

Reaktionsgleichung

Reaktionsgleichung von HRID 2290601
[NH2:1][C:2]1[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=1.[N:19]1[C:26](Cl)=[N:25][C:23](Cl)=[N:22][C:20]=1Cl.Cl>C1(C)C(C)=CC=CC=1>[CH2:9]([O:8][C:6]([C:5]1[CH:4]=[CH:3][C:2]([NH:1][N:19]2[CH2:26][N:25]([NH:1][C:2]3[CH:18]=[CH:17][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:4][CH:3]=3)[CH2:23][N:22]([NH:1][C:2]3[CH:3]=[CH:4][C:5]([C:6]([O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:7])=[CH:17][CH:18]=3)[CH2:20]2)=[CH:18][CH:17]=1)=[O:7])[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Komponenten

5

Edukt 3

HCID 313Hydrochloric AcidHCID 7954Cyanuric chlorideHCID 26629Octyl p-aminobenzoate

Produkt 1

HCID 201527331,3,5-Tris-(p-(oct-1-yloxycarbonyl)-anilino)-s-triazine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 7237O-XyleneLösungsmittel

Reaktionsbedingungen

Temperatur
90 °C

Versuchsvorschrift

75 g of octyl p-aminobenzoate and 18.5 g of cyanuric chloride in 1,000 ml of xylene were heated at 140° C. for 8 hours. After the evolution of hydrogen chloride was complete, the reaction solution was cooled to 90° C., washed twice with saturated sodium bicarbonate solution and once with water and then cooled to room temperature. The white crystals precipitated were filtered off under suction.

Aufarbeitung

  1. washwashed twice with saturated sodium bicarbonate solution and once with water
  2. temperaturecooled to room temperature
  3. customThe white crystals precipitated
  4. filtrationwere filtered off under suction

Quellen und Nachweise

ORD-Eintrag
ord-406a8ee66c394100acc9d9181a37e888
Quelldatensatz
uspto-grants-1986_10
Patentnummer
US04617390

Verknüpfte Notizen

Wird geladen…